Waterloo Advanced Technology Lab
http:// www.WATLab.com  or //leung.uwaterloo.ca/WATLab
University of Waterloo - Chemistry 2- 059-066/261 -  Tel: 519-888-4567 ext. 35826
Director - Professor Tong Leung
 
 
 

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What's New
Last Updated
2012-01-12 08:42
Contact us at:   manager @watlab.com  or director @watlab.com
Download a WATLab promo

 


 

 

 

12 Jan 12 *** Update on QNC tool acquisition and deployment.  - See message sent to WIN membership via WIN office on 3 Jan 12.- For more info, please contact Tong.

 

28 Apr 11 *** SEM resuming normal operation on 3 May 2011  A solid state relay on the vacuum board was found to be malfunctioning, which blocked the power up sequences of the foreline and  turbo pumps.  Jacek was able to replace this relay and we will be conducting machine physics for the rest of this week.  WATLab will resume normal SEM operation on Tuesday, May 3.

 

 

23 Apr 11 *** SEM Down until further notice  The LEO has suffered a vacuum problem and the foreline pump has problem starting up.  We are investigating the cause.  The system will be down until further notice.   Sorry for the inconvenience. 

 

22 Apr 11 *** ORION Plus ON-LINE  The ORION Plus Helium Ion Microscope has been installed in C2-080 and achieved spec-on-site (with 0.34 nm resolution) on 19 April, 2010.  We expect full operation within the next two months.

 

30 Mar 11 *** ORION Plus Helium Ion Microscope  Canada's very first Helium Ion Microscope will be installed in C2-080.  The new ion microscope is offering unprecedented spatial resolution of 0.35 nm with Z contrast for both hard and soft, conducting and nonconducting materials.  This unique tool is expected to put WATLab and uWaterloo at the cutting edge of microscopy research and nanosciences.

 

28 Mar 11 *** EBL Software upgrade:    A new version of the Nabity EBL software is being installed along with a new PC.  The EBL system will be down until further notice.  Sorry for the inconvenience.

 

 

 

BOOKING POLICY - "UPDATED" 29 May 2010

1.  RESERVE no more than TWO hours at a time and not exceeding SIX hours (total) a week.  Please reserve a realistic amount of time for a single time slot and be flexible with your start and end times to minimize gaps.  *** It's more efficient and less expensive for the user to run a few samples at the same time in a single time slot instead of one sample at a time in multiple time slots.

2.  ADVANCED BOOKING:  Not counting the time already reserved in the current week, individual users are allowed to make reservation not exceeding SIX hours (total and NOT per week) in no more than FOUR time slots in all of the coming weeks FOR GROUPS WITH MULTIPLE USERS: Please try NOT to block too many time slots so that other groups could have some access.  *** We will be removing any reservation exceeding TEN hours (total) or 5 time slots (maximum) from a single group.  Ten hours corresponds to one working day. 

3.  WALK-IN:  Please check the Bookit scheduler frequently, as time slots may become available due to schedule changes.  ***Unused time slots designated for Machine Physics and OS (and newly open-up Saturday time slots) will be released usually 24 hours in advance.

4.  CANCEL any reserved time slot at least THREE working days in advance so that other users can have a chance to book the free-up time.  *** Penalties for cancelling less than the 3 working days and for no show will be equivalent to OS service and industrial user rates respectively.

*** Penalty for not starting the session on time, i.e. within 10 minutes of the reserved start time, is OS service fee and loss of the reserved slot.

***No dirty hands, no food or no drink are allowed in the Lab during operation of the SEM.
***Penalty for spot-trading and letting uncertified users operate the machine is banishment.  Zero tolerance.

 

SEM FAQ-1:  How tight should the stub be tightened?  The machine shop has fixed the sample holder and now all eight positions work.  The problem was that the hex screw heads have been either all or partially stripped due to heavy tightening.  Please use only two fingers on the screw driver to tighten these screws.  It is NOT necessary to "crank" it down.  "Finger-tight" is enough to make good mechanical contact.  Tightening too much will not improve the SEM image and will only damage the screws and/or the sample stage.

SEM FAQ-2:  When taking the stubs out, please do NOT loosen the screws too much as they may fall off into the turbo pump below, killing everything!  We only need to loosen 1 to 2 turns, enough to take the stub out.

SEM FAQ-3:  Why should we care about how clean our sample is?  The cleanliness of the sample will affect the cleanliness of the chamber, which will in turn affect the performance of the machine.  Clearly any high-vapour pressure materials will not only make the vacuum bad but also coat the expensive EDX window and all the delicate SEM detectors inside, not to mention causing contamination to (and accelerate the death of) the expensive field-emission source and the lens stack.  Once the system is contaminated, there is virtually no way to clean the machine and it will be extremely expensive to do this.  The consequence is that EDX quantification, especially for low Z elements, will be way off and unreliable, and tons of carbon will appear in the SEM image during image acquisition.  Any user who doesn't respect the sample cleanliness rule will be banned from WATLab, as we don't want these users to ruin the machine for everyone.  Never just "think" it's OK to put your sample inside without checking with us first.  An "overconfident" user is the most dangerous one and is high-risk to other users.  Please exercise due caution, and have some respect for the machine and other WATLab users.  When in doubt, please come to ask us.  Please note that Mechanical Engineering Department (Professor Carolyn Hansson's group) has an Environmental SEM, which can accommodate high vapour-pressure materials.  For the FE-SEM in WATLab, we only want to deal with "clean" samples and low-risk users, as WATLab just doesn't have the cash to do any repair.

 

NEW services Now JN-LINE for high-resolution XRD and optical spectroscopies (UV/Vis, PL, Raman, FTIR).  Please contact us.

Looking for an exciting graduate or undergraduate research project in nanosciences and nanotechnology?  Please contact us at  tong@watlab.com  for further information. 
 

 

 
 

MICROSCOPY & LITHOGRAPHY
Chem-2 060 ext 33077

 

Scanning Electron Microscopy

LEO FESEM 1530 (with EDX/OIM)
Bookit

To request a user account - Download and complete the following Account Request Form for Academic Users Industrial Users.  For assistance and for the current rates for academic and industrial users, please contact us.

We now offer Operator Service, whereby our specialists will run the samples for the users (with the users present) and/or to train the user to eventually become a certified user.  The time allocated for Operator Service is normally Mon-Wed afternoon and by appointment with our specialist.  Certified users,*** who have been authorized by us to operate the machine on their own, can book the time directly online.  In the event of heavy booking, please allow for 3 working days for cancellation otherwise a penalty of 2 hours of SEM time will be charged.

All users are responsible for preparing their own samples.  For microscopy supplies (Cambridge stubs, double-sided conductive tapes, etc.), please contact SOQUELEC, Marivac, or Ted Pella.

*** To become a certified user, the new users should contact us to arrange for an initial training session (normally offered once a month).  SEM training will consist of watching a 20-minute on-line video about the general principle of SEM and other available facilities in the SEM lab, to be followed by a second hands-on training session (60-90 minutes) on how to operate the machines (at a charge of $50 per user).  New users must then attend a sufficient number (3-5) of Operator Service sessions so that we are confident that the user can handle the standard tasks.   [Download the on-line SEM Training Video Realmedia (38 MB) or Mpeg (172 MB) here.]

Specs and Specimen Stage - Look Inside
res1kv.tif res20kv.tif pb150375stage1.jpg pb150377stage3.jpg pb150376stage2.jpg pb150378stage4.jpg

 

 


For other microscopy and structural characterization tools available for Operator Service, please contact us.

Atomic Force Microscopy &


Pacific Nanotechnology
AFM Nano-R

Scanning Probe Microscopy &


Veeco DI Dimension 3100
Nanoscope IV

High Resolution X-ray Diffraction &

PANalytical MRD Xpert Pro 

 

 
 

SPECTROMICROSCOPY & SPECTROSCOPY
Chem-2 064 ext 33078
 

Imaging ESCA Microprobe
(X-ray Photoelectron Spectroscopy)



VG Scientific ESCALab 250

We are now accepting samples from the users for analysis on a cost-recovery basis.  Unlike the SEM, operation of the Imaging ESCA system is complex and delicate.  Only users with a solid background in UHV techniques will be trained on-site.  At 1.7 times the SEM rate, the service fee for using this unique state-of-the-art Imaging ESCA system has been made very competitive (for both commercial and academic users).  For information regarding the sample preparation requirements and to schedule a run, please contact us.

For XPS data analysis, we use CasaXPS.  To access CasaXPS, download the latest version from www.casaXPS.com .   Then, contact us to get the site-license password for the software (there will be a small fee to share the cost of the site license and we require the user to sign a copyright form).  To get started with CasaXPS, please study their help manual (Note the links: Quick Summary of Features, Converting File Formats (VG Advantage), Frequently Asked Questions, & Background Information to XPS), before contacting one of us.

 XPS Analyser - Look Inside
day11w31pb060353.jpg day11w31pb060354.jpg day11w31pb060358.jpg day11w31pb060360.jpg day11w31pb060365.jpg

Machine Physics
080111: Potential rate meter/slow-scanning problem

E250 Outside "Dizzy" Tour | E250 Behind-the-racks Tour
Test file


For other spectroscopy tools available for both Certified User and Operator Service, please contact us.

 

  • UV-Visible Spectroscopy: Perkin-Elmer Lambda 35 (with Lapshere integrating sphere optics for reflectance spectroscopy) 

  • Photoluminescence Spectroscopy:  Perkin-Elmer LS55 (with Xe lamp) 

  • Fourier-Transform Infrared Spectroscopy: Bruker Tensor 27 (with ATR and AGA optics) 

  • Raman Spectroscopy and Microscopy: Bruker Senterra Confocal Microscope (with 532 nm & 785 nm lasers) 

 

 
 

NANO-FABRICATION & MATERIALS SCIENCE
Chem-2 066 ext 36827
 

   

Tools being developed for general user service - more to come...
 

  • Electrodeposition & Quartz Crystal Microbalance

  • Monolayer films by Langmuir Blodgett Trough

  • Chemical Vapour Deposition

  • Pulsed Laser Deposition

  • Organic and Metal Molecular Beam Expitaxy

  • Ultrahigh Vacuum Surface Science Systems for TPD, XPS, IRAS, LEED/AES Studies Chem-2 061 ext 35827
     

  • Chemical Physics & Computer Modelling Chem-2 261 ext 35092

  • TEM Lab in Physics Phys 115 ext 33807

 
 

WATLab NEWS Archive
 

10 Jan 11 *** Messy workplace    After just one week from startup, we found that the sample prep hood was once again left with a big mess.  Once the entropy has started, the second law of thermodynamics will take over WATLab in no time.  We have implemented the following countermeasures:

 

1.  From now on, anyone caught leaving a big mess in the SEM, hood, gold coater, and other areas of WATLab will be charged a clean-up fee equivalent to 1 h of OS.   We will do a spot-check before and after each user's session to assure compliance.  As we just don't have human resource to clean up after these messy users, chronic messy users will be banished from WATLab altogether.  Each user MUST leave the workplace in a tidy and clean condition for the next user.

 

2.  Some users still don't know how to use the new system of the gold coater and proceed to unplug things on their own.  This is NOT acceptable.  If you have questions, please come to ask one of us.   If these users cannot follow the protocol, we will discontinue gold coating service at WATLab.

 

3 Jan 11 *** Happy New Year!   As we start this exciting new year (celebrating the International Year of Chemistry), we wish to draw your attention to the new booking system now in place (below).   In the interest of streamlining our operation, accounting and billing will only be done once a year (from April 2010 to February 2011) - please inform your boss and this will be done later in February.  WATLab will be completing all the upgrades to the SEM this term, including the upgrade to the Nabity EBL system.  WATLab is looking forward to the commissioning of the first Helium Ion Microscope in Canada (expected later in the spring) and of the first Secondary Ion Mass Spectrometry system on campus (expected later in the fall).  Various enhancements of our other materials science techniques will be made along the way, budget permitting.  With these new and upgraded existing tools, we hope that WATLab will continue to play a key role in enabling our users to engage in exciting new research in science and technology in Waterloo, Ontario, Canada, and beyond in 2011.  Happy data mining.

 

3 Dec 10 *** New SEM booking system now in place:  The Bookit system will be coming down on Dec 13.  WATLab will not move to its replacement (Outlook Exchange) b/c it's far too complicated to manage.  Instead, we will use google calendar. Beginning Dec 13, all SEM reservation will be made by logging in at:

 

http://calendar.google.com

 

Sign in with the login name   watlab.sem   and the appropriate password.  Certified users may obtain the new password from Nina.  As we are experimenting with this booking system, we wish to remind the user that the normal operating hours are 8 am to 4 pm, Monday to Friday.  We will block off Operator Service time slots once the system is stabilized.  We hope we could rely on all of our users to have some patience with each other as we go through this transition phase.  In the meantime, we take this opportunity to wish you all a happy holidays and all the best in 2011.

 

 

21 Oct 10 *** CCEM One-day Workshop:   There is a one-day microscopy workshop at Mac on Nov 5, 2010 (Friday).  Please see the workshop poster here

 

20 Oct 10 *** Computer security:  We are aware of the ongoing issues with the Raith EBL system at QNC.  This has been traced back to a USB stick of a user infected with the so-called "Chinese virus" that is known to infect not only the cpu of any computer but also any EPROM or processor in any electronic device (including all the electronic boards inside the SEM and virtually any machine systems at WATLab).  This type of virus is also very difficult to kill once it gets inside a "controller" as antivirus programs will not work with controllers without the proper OS.  This is a real and very potent threat and can serious damage not just all the computer systems and machines in WATLab but also all the computers of our entire user base and their groups.  We therefore ask all users to implement the following counter-measures:

 

1.  Do NOT use any of WATLab computers, including the USER DATA computer that stores the SEM images, for any email or messaging or internet or social networking activities.  Under no circumstances should any of the machine computers see the internet - do not run the browsers on these machines!  Anyone caught with using the browsers on these machines (including the SEM, EDX and EBL computers) will be banished forever from WATLab.  Please bring your own laptop for these activities and use wireless access.

 

2.  Do NOT bring in any old or suspect USB stick for transferring data.  Please RESERVE (and label) one new USB stick just for this purpose and don't use it for anything else.  WATLab will also provide blank DVD for writing data, if needed.  The idea is to minimize exposure of our systems to the external world.

 

3.  Please report to us ANY user activity that does not follow these simple rules.  I think we all agree that it is of everyone's interest to protect WATLab's systems because once affected they will become the point of infection that spreads the virus to all the computers of anyone who uses WATLab.  This could affect us all very negatively, especially our graduate students who may be writing their theses.

 

Thank you for your continued cooperation.

 

11 Oct 10 *** EBL upgrade & spectroscopy fleet relocation: There will be a software (to Version 9 and XP) and hardware upgrade (control board) to the Nabity EBL system, which will improve the write speed and off-line design flexibility.  We will implement this change during machine physics time slots and hopefully with minimal service interruption.

WATLab is expanding into some recently found space to accommodate the two new instrument clusters and the RPL.  We will also be able to relocate the spectroscopy fleet to this new space before Christmas.  We expect this should relieve the severe space shortage experienced in all areas of WATLab.

 

 3 Sept 10 *** Normal operation: As we begin a very busy fall term, we wish to again remind the user of the heavy fines for late start and no show.  Please have your sample in hand before making machine reservation to avoid these penalties.  Please also note that we have made an adjustment to the gold coating cost due to the sharp rise in gold prices and added a surcharge to those who just use our gold coater and not our SEM.

 

22 July 10 *** Vacuum problem:We have located the leak and removed this problem temporarily.  A new vacuum readout problem has emerged and we have been working on this last week.  We don't think we have completely resolved this issue but we will resume normal service starting July 23.  Thank you for our patience.

 

6 July 10 *** Vacuum problem:The chamber pressure has become very poor.  We have replaced the turbo but the problem remains.  We are in contact with the service engineer to find a fix.  System will be down until further notice.  Please watch the bookit scheduler.

 

5 July 10 *** Stage fixed, but what a messy workplace:  The stage issue has been fixed for now.  The system will be available by noon.

 

But I found the clean hood and the SEM general area are always left in a big mess!  I spent 20 minutes cleaning this up this morning and we will not do this again.  From now on, we will check the lab condition after each user has completed the session.  If we find the workplace is left in a messy and disorganized condition, we will charge a lab cleanup fee ($50) to the user.  Please treat your fellow user with some respect and leave a clean, tidy and pleasant work environment for the next user.  Thank you very much for your cooperation.

4 July 10 *** Stage failure:  The stage cannot be initialized in the X-Y plane and we cannot use the system until further notice.  We are investigating the cause of the failure.

26 June 10 *** Upgrade complete:  The various upgrades for the SEM/EDX/OIM systems are finally complete.  Zeiss has fixed the miscellaneous air-jack problem and has also replaced the power control board (that gave the 24 V error).  We don't expect any more service interruption until the filament dies.  Our backlog appears to be improving (down to 2 weeks).

 

4 June 10 *** No show and cancellation:  We notice a large number of recent no shows and last-minute cancellations.  Please note that there will be heavy fines equivalent to the OS rate ($70/h) or industrial user rate ($165/h) and we will start informing your boss.  Have some respect for other users who may need the time.  We need THREE working days for cancellation.  Do not book the machine unless you have samples in hand.

 

29 May 10 *** SEM normal operation:   Backlog is coming down to acceptable level (2 weeks).  Filament is on its last legs.  Expect filament replacement soon and minor service interruption to repair vibration membranes in the next 2-3 months.

 

31 Mar 10 *** SEM resuming normal operation:   The brief SEM pc problem (file saving issue) that one user encountered this afternoon has been resolved and we are resuming normal operation.  I'll be on site on this good Friday for those users who decide to do data mining that day.  Happy Easter.

 

21 May 10 *** Victoria Day Monday:   WATLab will be open and on normal operation on Monday 24 May 2010.

 

12 Mar 10 *** Carbon coating:   Those users doing the carbon coating are always leaving the station in a big mess and creating dangerous situation by not turning off the controller after use.  WATLab will withdraw this self-serve service.  Effectively immediately, users who will need to have their samples C-coated should submit their samples 5 working days in advance, and we will do this service for them at a charge of $50 per coating.

 

17 Feb 10 *** Spot trading:   WATLab continues to have problems with a few users not following the booking rules.  We found some of these users are starting to trade their spots with other users.  This is forbidden because the facility needs to track the machine usage in case of system breakdown.  If the user starts trading booking spots, then we will lose track of the responsible party and the type of samples that may be causing the machine problems.  This is also the reason why each user must be trained and certified individually.  There is no substitution.  From now on, users caught trading their spots will be denied access and their entire group will also be denied access.  Zero tolerance.

 

Given that WATLab does not have an army of facility staff to monitor the usage and is essentially a self-serve honour system, we hope that the user will understand that these "strict" facility rules are there to protect the machines and the general user community.  If we allow individual users to set their own rules as they please, the facility integrity will degrade quickly, which will lead to chaos that is ultimately bad for all users.

 

12 Feb 10 *** Fines for no-show doubled:   This morning, both users did not show up for their appointed time slots.  You know who you are!  This is a clear sign of lack of respect for other users, especially when we are all trying to get some time on the machine to do some work.  We have now DOUBLED the fines for no-show (i.e. twice the rate of OS = $140 per hour) and your boss will be notified.  Please remember that we require 3 working days for cancellation so that other users can rebook (it's no good if you cancel in the last minute as the time will still be wasted).  If the present countermeasure does not work, these "no-show" users will be denied future access and they will be off our grid permanently.

 

27 Jan 10 *** Booking rules and backlog:   Due to the recent surge in the SEM usage, we wish to remind everyone to treat your fellow user and the machine with respect and to observe the following protocols:

1.  Please observe the booking rules, i.e. not counting the current week, reserve in the coming weeks no more than SIX hours total in no more than FOUR time slots.  THIS MEANS: A user should reserve, in ALL of the coming weeks not counting the present week (and not per week), the total amount of time not more than 6 hours and the number of time slots not more than 4, whichever is less.  We will be monitoring this closely and implement heavy fines for users who overbook.  Users who continue to ignore the booking rules will be blocked.

2.  Please show up on time and do not book a time period longer than you need.  There will be fines for users who show up late.  Also, try not to leave too many gaps in between time slots.

3.  The fine for "no-show" is charges equivalent to hours for OS industrial rate, and we will start indicating this on our accounting statement to your boss - this means your boss will know.  We require 3 working days for cancellation to allow other users to re-book.

4.  We will be creating a new class of users to allow these "senior users" to access evening and Saturday time slots (when they become available).  Only the most responsible "permanent" users will be given this privilege.

5.  If all these measures do not work, then we will start blocking all undergraduate users from WATLab.

 

11 Dec 09 *** ORF announcement at WATLab:  Full story at TheRecord.com

 

WATLab FAQ

For more info
contact tong @watlab.com

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